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文献信息

Multi-walled Carbon Nanotubes-Aminate Reduced Graphene Oxide Modified Glassy Carbon Electrode as the Voltammetric Sensor for Sensitive Electrochemical Determination of Rutin

期刊名:INT J ELECTROCHEM SC
文献编号:
文献地址: http://www.electrochemsci.org/papers/vol10/101109192.pdf
发表日期:Oct 2015

Multi-walled Carbon Nanotubes-Aminate Reduced Graphene Oxide Modified Glassy Carbon Electrode as the Voltammetric Sensor for Sensitive Electrochemical Determination of Rutin

Xiaofei Zhu , Jingkun Xu, Xuemin Duan, Limin Lu, Huakun Xing , Yansha Gao, Hui Sun, Liqi Dong,Taotao Yang

Abstract

In this paper, a highly sensitive voltammetric method for determination of rutin is developed using multi-walled carbon nanotubes-aminate reduced graphene oxide (MWCNTs/ARGO) modified electrode. The incorporated ARGO served as dispersing agent and conductive sheet, which could effectively prevented aggregation of MWCNTs. Compared with either MWCNTs or ARGO, the hybrid nanomaterials showed a strong synergistic effect between two materials and exhibited higher activity for the electro-oxidation of rutin. MWCNTs/ARGO composite was characterized by scanning electron microscope (SEM) and electrochemical impedance spectroscopy (EIS). Under the optimized conditions, MWCNTs/ARGO modified electrode exhibited wide linear range from 0.01 to 112 M with the detection limit of 2 nM (S/N = 3). Moreover, the proposed method was successfully applied to determine rutin in compound rutin tablets and satisfactory results were obtained.

Chemicals and reagents Rutin was obtained from Biopurify?.

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